Table 1.
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Parameters of DSC analysis.

InstrumentSample panProcedure for DSCProcedure for mDSCPurge gasFlow rate
TA, Discovery DSC 250Aluminum, pin-holedEquilibrate 25 °C
Ramp 10 °C/min to 300 °C		Data Off: Equilibrate −30 °C
Modulate Template 0.64 °C for 120.0 s
Isothermal 10.0 min
Data On: Ramp 2 °C/min to 300 °C		N250 ml/min
InstrumentSample panProcedure for DSCProcedure for mDSCPurge gasFlow rate
TA, Discovery DSC 250Aluminum, pin-holedEquilibrate 25 °C
Ramp 10 °C/min to 300 °C		Data Off: Equilibrate −30 °C
Modulate Template 0.64 °C for 120.0 s
Isothermal 10.0 min
Data On: Ramp 2 °C/min to 300 °C		N250 ml/min
Table 1.
Open in new tab

Parameters of DSC analysis.

InstrumentSample panProcedure for DSCProcedure for mDSCPurge gasFlow rate
TA, Discovery DSC 250Aluminum, pin-holedEquilibrate 25 °C
Ramp 10 °C/min to 300 °C		Data Off: Equilibrate −30 °C
Modulate Template 0.64 °C for 120.0 s
Isothermal 10.0 min
Data On: Ramp 2 °C/min to 300 °C		N250 ml/min
InstrumentSample panProcedure for DSCProcedure for mDSCPurge gasFlow rate
TA, Discovery DSC 250Aluminum, pin-holedEquilibrate 25 °C
Ramp 10 °C/min to 300 °C		Data Off: Equilibrate −30 °C
Modulate Template 0.64 °C for 120.0 s
Isothermal 10.0 min
Data On: Ramp 2 °C/min to 300 °C		N250 ml/min
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